[1] Scientific Working Group for Forensic Toxicology, Scientific Working Group for Forensic Toxicology
(SWGTOX) Standard Practices for Method Validation in Forensic Toxicology, Journal of Analytical
Toxicology 37 (2013) 452–474.
[2] Pirro, Valentina and Valente, Valeria and Oliveri, Paolo and De Bernardis, Angela and Salomone,
Alberto and Vincenti, Marco, Chemometric evaluation of nine alcohol biomarkers in a large population
of clinically-classified subjects: pre-eminence of ethyl glucuronide concentration in hair for
confirmatory classification, Analytical and Bioanalytical Chemistry 401 (2011) 2153.
[3] Fulgoni III, Victor L and Keast, Debra R and Lieberman, Harris R, Trends in intake and sources
of caffeine in the diets of US adults: 2001–2010, The American Journal of Clinical Nutrition 101
(2015) 1081–1087.
[4] Andresen-Streichert, Hilke and M¨uller, Alexander and Glahn, Alexander and Skopp, Gisela and
Sterneck, Martina, Alcohol biomarkers in clinical and forensic contexts, Deutsches ¨Arzteblatt
International 115 (2018) 309.
[5] N. C. for Health Statistics, National health and nutrition examination survey. hyattsville, md: U.s.
department of health and human services, centers for disease control and prevention, 2018.
[6] Elliott, Simon and Smith, Christopher and Cassidy, Diane, The post-mortem relationship between
beta-hydroxybutyrate (BHB), acetone and ethanol in ketoacidosis, Forensic Science International
198 (2010) 53–57.
[7] Osuna, Eduardo and Vivero, Guillermo and Conejero, Josefa and Abenza, Jos´e M and Mart´ınez,
Pedro and Luna, Aurelio and P´erez-C´arceles, Mar´ıa D, Postmortem vitreous humor β-
hydroxybutyrate: its utility for the postmortem interpretation of diabetes mellitus, Forensic Science
International 153 (2005) 189–195.
[8] Hess, Cornelius and Sydow, Konrad and Kueting, Theresa and Kraemer, Michael and Maas, Alexandra,
Considerations regarding the validation of chromatographic mass spectrometric methods for
the quantification of endogenous substances in forensics, Forensic Science International 283 (2018)
150–155.
[9] Wille, Sarah MR and Peters, Frank T and Di Fazio, Vincent and Samyn, Nele, Practical aspects
concerning validation and quality control for forensic and clinical bioanalytical quantitative
methods, Accreditation and Quality Assurance 16 (2011) 279.
[10] Skoog, Douglas A., Holler, F. James, Crouch, Stanley R., Selecting an Analytical Method, in:
Principles of Instrumental Analysis, Cengage Learning, Belmont, United States, 6 edition, 2006,
pp. 17–21.
[11] Elliott, Simon P, Gamma hydroxybutyric acid (GHB) concentrations in humans and factors affecting
endogenous production, Forensic Science International 133 (2003) 9–16.
[12] Jemal, Mohammed and Schuster, Alan and Whigan, Daisy B, Liquid chromatography/tandem
mass spectrometry methods for quantitation of mevalonic acid in human plasma and urine: method
validation, demonstration of using a surrogate analyte, and demonstration of unacceptable matrix
effect in spite of use of a stable isotope analog internal standard, Rapid Communications in Mass
Spectrometry 17 (2003) 1723–1734.
[13] Ji, Dajeong and Jang, Choon-Gon and Lee, Sooyeun, A sensitive and accurate quantitative method
to determine N-arachidonoyldopamine and N-oleoyldopamine in the mouse striatum using columnswitching
LC–MS–MS: use of a surrogate matrix to quantify endogenous compounds, Analytical
and Bioanalytical Chemistry 406 (2014) 4491–4499.
[14] Jones, Barry R and Schultz, Gary A and Eckstein, James A and Ackermann, Bradley L, Surrogate
matrix and surrogate analyte approaches for definitive quantitation of endogenous biomolecules,
Bioanalysis 4 (2012) 2343–2356.
[15] Binz, Tina M and Braun, Ueli and Baumgartner, Markus R and Kraemer, Thomas, Development
of an LC–MS/MS method for the determination of endogenous cortisol in hair using 13C3-labeled
cortisol as surrogate analyte, Journal of Chromatography B 1033 (2016) 65–72.
[16] Kang, Soyoung and Oh, Seung Min and Chung, Kyu Hyuck and Lee, Sooyeun, A surrogate analytebased
LC–MS/MS method for the determination of γ-hydroxybutyrate (GHB) in human urine and
variation of endogenous urinary concentrations of GHB, Journal of Pharmaceutical and Biomedical
Analysis 98 (2014) 193–200.
[17] Savard, St´ephanie and Lapointe, Christine and Lamarche, Martine and Mireault, Pascal, Development
of a new method for simultaneous quantitative BHB and GHB analysis by GC-MS, Standard,
Poster presented at the International Association of Forensic Sciences (IAFS) 2017 Meeting,
Toronto, Canada, 2017.
[18] Thermo Scientific, Instructions.: BSTFA + TMCS N,O-bis(Trimethylsilyl)trifluoroacetamide with
Trimethylchlorosilane, Standard, https://fscimage.fishersci.com/images/D00369 .pdf (Retrieved
January 28th 2018), 2017.
[19] ISO/IEC 17025:2005, General requirements for the competence of testing and calibration laboratories,
Standard, International Organization for Standardization, Geneva, Switzerland, 2005.
[20] CAN-P-1578, Guidelines for the Accreditation of Forensic Testing Laboratories, Standard, Standards
Council of Canada (Conseil canadien des normes), Ottawa, Canada, 2009.
[21] Desharnais, Brigitte and Camirand-Lemyre, F´elix and Mireault, Pascal and Skinner, Cameron D,
Procedure for the Selection and Validation of a Calibration Model I — Description and Application,
Journal of Analytical Toxicology 41 (2017) 261–268.
[22] Desharnais, Brigitte and Camirand-Lemyre, F´elix and Mireault, Pascal and Skinner, Cameron D,
Procedure for the Selection and Validation of a Calibration Model II — Theoretical Basis, Journal
of Analytical Toxicology 41 (2017) 269–276.
[23] D.L. Massart, B.G.M. Vandeginste, L.M.C Buydens, S. De Jong, P.J. Lewi, J. Smeyers-Verbeke,
Straight Line Regression and Calibration, in: Handbook of Chemometrics and Qualimetrics: Part
A, volume 20A of Data Handling in Science and Technology, Elsevier, Amsterdam, Netherlands,
1997, pp. 171–230.
[24] Navidi, William, Propagation of Error, in: Statistics for Engineers and Scientists, Mc Graw Hill
Education, New York, United States, 2014, pp. 164–199.
[25] Z¨orntlein, SW and Kopp, A and Becker, Julie and Kaufmann, TJ and R¨ohrich, J and Urban, R,
In vitro production of GHB in blood and serum samples under various storage conditions, Forensic
Science International 214 (2012) 113–117.