Seede, Raiyan, Mostafa, Ahmad ORCID: https://orcid.org/0000-0001-5625-1106, Vladimir, Brailovski, Mohammad, Jahazi and Medraj, Mamoun (2018) Microstructural and Microhardness Evolution from Homogenization and Hot Isostatic Pressing on Selective Laser Melted Inconel 718: Structure, Texture, and Phases. Journal of Manufacturing and Materials Processing, 2 (2). p. 30. ISSN 2504-4494
Preview |
Text (Publisher version) (application/pdf)
9MBjmmp-02-00030.pdf - Published Version Available under License Creative Commons Attribution. |
Official URL: http://www.mdpi.com/2504-4494/2/2/30/htm
Abstract
In this work, the microstructure, texture, phases, and microhardness of 45° printed (with respect to the build direction) homogenized, and hot isostatically pressed (HIP) cylindrical IN718 specimens are investigated. Phase morphology, grain size, microhardness, and crystallographic texture at the bottom of each specimen differ from those of the top due to changes in cooling rate. High cooling rates during the printing process generated a columnar grain structure parallel to the building direction in the as-printed condition with a texture transition from (001) orientation at the bottom of the specimen to (111) orientation towards the specimen top based on EBSD analysis. A mixed columnar and equiaxed grain structure associated with about a 15% reduction in texture is achieved after homogenization treatment. HIP treatment caused significant grain coarsening, and engendered equiaxed grains with an average diameter of 154.8 µm. These treatments promoted the growth of δ-phase (Ni3Nb) and MC-type brittle (Ti, Nb)C carbides at grain boundaries. Laves phase (Fe2Nb) was also observed in the as-printed and homogenized specimens. Ostwald ripening of (Ti, Nb)C carbides caused excessive grain growth at the bottom of the HIPed IN718 specimens, while smaller grains were observed at their top. Microhardness in the as-fabricated specimens was 236.9 HV and increased in the homogenized specimens by 19.3% to 282.6 HV due to more even distribution of secondary precipitates, and the nucleation of smaller grains. A 36.1% reduction in microhardness to 180.5 HV was found in the HIPed condition due to phase dissolution and differences in grain morphology.
Divisions: | Concordia University > Gina Cody School of Engineering and Computer Science > Mechanical, Industrial and Aerospace Engineering |
---|---|
Item Type: | Article |
Refereed: | Yes |
Authors: | Seede, Raiyan and Mostafa, Ahmad and Vladimir, Brailovski and Mohammad, Jahazi and Medraj, Mamoun |
Journal or Publication: | Journal of Manufacturing and Materials Processing |
Date: | 16 May 2018 |
Funders: |
|
Digital Object Identifier (DOI): | 10.3390/jmmp2020030 |
Keywords: | Inconel 718; additive manufacturing; 3D printing; selective laser melting (SLM); hot isostatic pressing (HIP); homogenization; hardness; precipitation; microstructure; texture |
ID Code: | 983890 |
Deposited By: | AHMAD MOSTAFA |
Deposited On: | 22 May 2018 13:19 |
Last Modified: | 22 May 2018 13:19 |
Related URLs: |
References:
Wang, X.; Gong, X.; Chou, K. Review on Powder-Bed Laser Additive Manufacturing of Inconel 718 Parts. Proc. Inst. Mech. Eng. Part B J. Eng. Manuf. 2017, 231.Jia, Q.; Gu, D. Selective laser melting additive manufacturing of Inconel 718 superalloy parts: Densification, microstructure and properties. J. Alloy. Compd. 2014, 585, 713–721.
Qi, H.; Azer, M.; Ritter, A. Studies of standard heat treatment effects on microstructure and mechanical properties of laser net shape manufactured INCONEL 718. Metall. Mater. Trans. A Phys. Metall. Mater. Sci. 2009, 40, 2410–2422.
Wang, Z.; Guan, K.; Gao, M.; Li, X.; Chen, X.; Zeng, X. The microstructure and mechanical properties of deposited-IN718 by selective laser melting. J. Alloy. Compd. 2012, 513, 518–523.
Debarbadillo, J.J.; Mannan, S.K. Alloy 718 for oilfield applications. JOM 2012, 64, 265–270.
Izquierdo, B.; Plaza, S.; Sánchez, J.A.; Pombo, I.; Ortega, N. Numerical prediction of heat affected layer in the EDM of aeronautical alloys. Appl. Surf. Sci. 2012, 259, 780–790.
Yap, C.Y.; Chua, C.K.; Dong, Z.L.; Liu, Z.H.; Zhang, D.Q.; Loh, L.E.; Sing, S.L. Review of selective laser melting: Materials and applications. Appl. Phys. Rev. 2015, 2.
Hague, R.; Campbell, I.; Dickens, P. Implications on design of rapid manufacturing. Proc. Inst. Mech. Eng. Part C J. Mech. Eng. Sci. 2003, 217, 25–30.
Campbell, R.I.; Hague, R.J.; Sener, B.; Wormald, P.W. The Potential for the Bespoke Industrial Designer. Des. J. 2003, 6, 24–34.
Choi, J.P.; Shin, G.H.; Yang, S.; Yang, D.Y.; Lee, J.S.; Brochu, M.; Yu, J.H. Densification and microstructural investigation of Inconel 718 parts fabricated by selective laser melting. Powder Technol. 2017, 310, 60–66.
Amato, K.N.; Gaytan, S.M.; Murr, L.E.; Martinez, E.; Shindo, P.W.; Hernandez, J.; Collins, S.; Medina, F. Microstructures and mechanical behavior of Inconel 718 fabricated by selective laser melting. Acta Mater. 2012, 60, 2229–2239.
Chlebus, E.; Gruber, K.; Kuźnicka, B.; Kurzac, J.; Kurzynowski, T. Effect of heat treatment on the microstructure and mechanical properties of Inconel 718 processed by selective laser melting. Mater. Sci. Eng. A 2015, 639, 647–655.
Mostafa, A.; Rubio, I.P.; Brailovski, V.; Jahazi, M.; Medraj, M. Structure, texture and phases in 3D printed IN718 alloy subjected to homogenization and HIP treatments. Metals 2017, 7, 196.
Thijs, L.; Sistiaga, M.L.M.; Wauthle, R.; Xie, Q.; Kruth, J.P.; van Humbeeck, J. Strong morphological and crystallographic texture and resulting yield strength anisotropy in selective laser melted tantalum. Acta Mater. 2013, 61, 4657–4668.
Segersäll, M.; Moverare, J.J. Crystallographic orientation influence on the serrated yielding behavior of a single-crystal superalloy. Materials 2013, 6, 437–444.
Segersäll, M.; Moverare, J.J.; Simonsson, K.; Johansson, S. Deformation and damage mechanisms during thermomechanical fatigue of a single-crystal superalloy in the and directions. Superalloys 2012, 215–223.
Popovich, V.A.; Borisov, E.V.; Heurtebise, V.; Riemslag, T.; Popovich, A.A.; Sufiiarov, V.S. Creep and Thermomechanical Fatigue of Functionally Graded Inconel 718 Produced by Additive Manufacturing. In TMS 2018 147th Annual Meeting & Exhibition Supplemental Proceedings; Springer: Berlin/Heidelberg, Germany, 2018; pp. 85–97.
Parimi, L.L.; Ravi, G.; Clark, D.; Attallah, M.M. Microstructural and texture development in direct laser fabricated IN718. Mater. Charact. 2014, 89, 102–111.
Zhang, D.; Niu, W.; Cao, X.; Liu, Z. Effect of standard heat treatment on the microstructure and mechanical properties of selective laser melting manufactured Inconel 718 superalloy. Mater. Sci. Eng. A 2015, 644, 32–40.
Tucho, W.M.; Cuvillier, P.; Sjolyst-Kverneland, A.; Hansen, V. Microstructure and hardness studies of Inconel 718 manufactured by selective laser melting before and after solution heat treatment. Mater. Sci. Eng. A 2017, 689, 220–232.
EOS Gmbh Electro Optical Systems. EOS Nickelalloy Inconel 718 Datasheet; EOS Gmbh: Krailling, Germany, 2014.
Smith, D.H.; Bicknell, J.; Jorgensen, L.; Patterson, B.M.; Cordes, N.L.; Tsukrov, I.; Knezevic, M. Microstructure and mechanical behavior of direct metal laser sintered Inconel alloy 718. Mater. Charact. 2016, 113, 1–9.
Rasband, W.S. ImageJ; U. S. National Institutes of Health: Bethesda, MD, USA, 2012. Available online: https://imagej.nih.gov/ij/ (accessed on 16 May 2018).
Degen, T.; Sadki, M.; Bron, E.; König, U.; Nénert, G. The HighScore suite. Powder Diffr. 2014, 29, S13–S18.
Pierre, V. Pearson’s Crystal Data, Crystal Structure Database for Inorganic Compounds (on CD-ROM); ASM International: Materials Park, OH, USA, 2010.
Campanelli, S.L.; Casalino, G.; Contuzzi, N.; Ludovico, A.D. Taguchi optimization of the surface finish obtained by laser ablation on selective laser molten steel parts. Procedia CIRP 2013, 12, 462–467.
Kasperovich, G.; Haubrich, J.; Gussone, J.; Requena, G. Correlation between porosity and processing parameters in TiAl6V4 produced by selective laser melting. Mater. Des. 2016, 105, 160–170.
Ali, H.; Ma, L.; Ghadbeigi, H.; Mumtaz, K. In-situ residual stress reduction, martensitic decomposition and mechanical properties enhancement through high temperature powder bed pre-heating of Selective Laser Melted Ti6Al4V. Mater. Sci. Eng. A 2017, 695, 211–220.
Agius, D.; Kourousis, K.; Wallbrink, C. A Review of the As-Built SLM Ti-6Al-4V Mechanical Properties towards Achieving Fatigue Resistant Designs. Metals 2018, 8, 75.
Popovich, V.A.; Borisov, E.V.; Popovich, A.A.; Sufiiarov, V.S.; Masaylo, D.V.; Alzina, L. Functionally graded Inconel 718 processed by additive manufacturing: Crystallographic texture, anisotropy of microstructure and mechanical properties. Mater. Des. 2017, 114, 441–449.
Zheng, L.; Liu, Y.; Sun, S.; Zhang, H. Selective laser melting of Al-8.5Fe-1.3V-1.7Si alloy: Investigation on the resultant microstructure and hardness. Chin. J. Aeronaut. 2015, 28, 564–569.
Zhou, X.; Li, K.; Zhang, D.; Liu, X.; Ma, J.; Liu, W.; Shen, Z. Textures formed in a CoCrMo alloy by selective laser melting. J. Alloy. Compd. 2015, 631, 153–164.
Liu, L.; Zhai, C.; Lu, C.; Ding, W.; Hirose, A.; Kobayashi, K.F. Study of the effect of Delta phase on hydrogen embrittlement of Inconel 718 by notch tensile tests. Corros. Sci. 2005, 47, 355–367.
Koul, A.K.; Au, P.; Bellinger, N.; Thamburaj, R.; Wallace, W.; Immarigeon, J.P. Development of a Damage Tolerant Microstructure for Inconel 718 Turbine Disc Material. Superalloys 1988, 3–10.
Rao, G.A.; Kumar, M.; Srinivas, M.; Sarma, D.S. Effect of solution treatment temperature on microstructure and mechanical properties of hot isostatically pressed superalloy Inconel 718. Mater. Sci. Technol. 2004, 20, 1161–1170.
Mitchell, A.; Schmalz, A.J.; Schvezov, C.; Cockcroft, S.L. The Precipitation of Primary Carbides in Alloy 718. Superalloys 1994, 65–78.
Kuo, Y.-L.; Kakehi, K. Influence of Powder Surface Contamination in the Ni-Based Superalloy Alloy718 Fabricated by Selective Laser Melting and Hot Isostatic Pressing. Metals 2017, 7, 367.
Murr, L.E.; Martinez, E.; Gaytan, S.M.; Ramirez, D.A.; MacHado, B.I.; Shindo, P.W.; Martinez, J.L.; Medina, F.; Wooten, J.; Ciscel, D.; et al. Microstructural architecture, microstructures, and mechanical properties for a nickel-base superalloy fabricated by electron beam melting. Metall. Mater. Trans. A Phys. Metall. Mater. Sci. 2011, 42, 3491–3508.
Murr, L.E.; Martinez, E.; Amato, K.N.; Gaytan, S.M.; Hernandez, J.; Ramirez, D.A.; Shindo, P.W.; Medina, F.; Wicker, R.B. Fabrication of metal and alloy components by additive manufacturing: Examples of 3D materials science. J. Mater. Res. Technol. 2012, 1, 42–54.
Donachie, M.J.; Donachie, S.J. Superalloys: A Technical Guide, 2nd ed.; ASM International: Geauga County, OH, USA, 2002.
Muralidharan, B.G.; Shankar, V. Weldability of Inconel 718—A Review; Indira Gandhi Centre for Atomic Research: Tamil Nadu, India, 1996; pp. 1–30.
Manikandan, S.G.K.; Sivakumar, D.; Rao, K.P.; Kamaraj, M. Laves phase in alloy 718 fusion zone—Microscopic and calorimetric studies. Mater. Charact. 2015, 100, 192–206.
Azadian, S.; Wei, L.Y.; Warren, R. Delta phase precipitation in inconel 718. Mater. Charact. 2004, 53, 7–16.
Idell, Y.; Levine, L.E.; Allen, A.J.; Zhang, F.; Campbell, C.E.; Olson, G.B.; Gong, J.; Snyder, D.R.; Deutchman, H.Z. Unexpected δ-phase formation in additive-manufactured Ni-based superalloy. JOM 2016, 68, 950–959.
Jouiad, M.; Marin, E.; Devarapalli, R.S.; Cormier, J.; Ravaux, F.; le Gall, C.; Franchet, J.M. Microstructure and mechanical properties evolutions of alloy 718 during isothermal and thermal cycling over-aging. Mater. Des. 2016, 102, 284–296.
Sjoberg, G.; Ingesten, N.G.; Carlson, R.G. Grain Boundary δ-phase Morphologies. Carbides and Notch Rupture Sensitivity of Cast Alloy 718. Superalloys 1991.
Maity, T.; Chawake, N.; Kim, J.T.; Eckert, J.; Prashanth, K.G. Anisotropy in local microstructure—Does it affect the tensile properties of the SLM samples? Manuf. Lett. 2018, 15, 33–37.
Repository Staff Only: item control page